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Selective manipulation of steroid hydroxyl groups with boronate esters: efficient access to antigenic C-3 linked steroid-protein conjugates and steroid sulfate standards for drug detection

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Date

2006

Authors

Hungerford, Natasha
McKinney, Andrew
Stenhouse, Allen M
McLeod, Malcolm

Journal Title

Journal ISSN

Volume Title

Publisher

Royal Society of Chemistry

Abstract

The temporary protection of 17α-alkyl-5α-androstane-3β, 16β,17β triols as boronate esters is an efficient method for their regioselective functionalisation. This has been applied to the synthesis of protein-steroid conjugates 7-10 suitable for the de

Description

Keywords

Keywords: Antigens; Bioassay; Biosynthesis; Drug therapy; Esters; Immunology; Proteins; Boronate esters; Drug detection; Immunoassays; Steroid hydroxyl groups; Hormones; antigen; boron derivative; ester; hydroxyl radical; oxosteroid; protein; steroid; sulfate; arti

Citation

URI

http://hdl.handle.net/1885/52849

Collections

Open Access Research

Source

Organic and Biomolecular Chemistry

Type

Journal article

Book Title

Entity type

Access Statement

License Rights

DOI

10.1039/b610499a

Restricted until

2037-12-31

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Description
01_Hungerford_Selective_manipulation_of_2006.pdf (281.99 KB)

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