Test environment running 7.6.6

Cultural advice

The Australian National University acknowledges, celebrates and pays our respects to the Ngunnawal and Ngambri people of the Canberra region and to all First Nations Australians on whose traditional lands we meet and work, and whose cultures are among the oldest continuing cultures in human history.

Aboriginal and Torres Strait Islander peoples are advised that ANU Library collections may include images, names, voices, and other representations of deceased persons.

Material in the collection may contain terms, language or views that reflect the period in which the item was created and may be considered inappropriate today.

Stereoselective synthesis of glycosyl acrylate derivatives by microwave assisted Wittig reaction

Thumbnail Image

Date

2012

Authors

Journal Title

Journal ISSN

Volume Title

Publisher

Abstract

In order to develop an efficient, practical and stereoselective method for synthesizing glycosyl acrylate derivatives, the microwave assisted Wittig reaction of sugar ketone(1) and lactones(4) with ylide 2(Ph 3P[CDS1]CHCOOEt) was investigated in a sealed microwave reactor in various temperatures and solvents. The reaction was carried out effectively and stereoselectively in xylene at 180°C with a yield up to 80% within 10 min.

Description

Keywords

Glycosyl acrylate derivative, Microwave assisted reaction, Stereoselective synthesis, Wittig reaction

Citation

URI

https://dspace-test.anu.edu.au/handle/1885/733729839

Collections

DevOps Pure Testing

Source

Kao Teng Hsueh Hsiao Hua Heush Hsueh Pao/ Chemical Journal of Chinese Universities

Type

Article

Book Title

Entity type

Access Statement

License Rights

DOI

10.3969/j.issn.0251-0790.2012.05.017

Restricted until

DSpace software copyright © 2002-2026 LYRASIS