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Resolution of (±)-nipecotic acid ((±)-3-piperidinecarboxylic acid) by separation of palladium(II) diastereomers containing orthometallated (S)-(-)-1-[1-(dimethylamino)ethyl]naphthalene

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Date

2008

Authors

Gugger, Paul
Hockless, David
Kilah, Nathan
Mayadunne, Roshan
Wild, Stanley (Bruce)

Journal Title

Journal ISSN

Volume Title

Publisher

Pergamon-Elsevier Ltd

Abstract

An efficient resolution of (±)-nipecotic acid has been achieved by the fractional crystallization of internally diastereomeric palladium(II) complexes containing the chelated carboxylate and orthometallated (S)-(-)-1-[1-(dimethylamino)ethyl]naphthalene.

Description

Keywords

Keywords: 1 [1 (dimethylamino)ethyl]naphthalene; hydrochloric acid; naphthalene derivative; nipecotic acid; nipecotic acid (3 piperidinecarboxylic acid); palladium; article; chemical structure; crystallization; enantiomer; priority journal; proton nuclear magnetic

Citation

URI

http://hdl.handle.net/1885/54028

Collections

Open Access Research

Source

Tetrahedron: Asymmetry

Type

Journal article

Book Title

Entity type

Access Statement

License Rights

DOI

10.1016/j.tetasy.2008.07.018

Restricted until

2037-12-31

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Description
01_Gugger_Resolution_of_(±)-nipecotic_2008.pdf (203.45 KB)

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