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Microwave assisted 1,3-dipolar cycloaddition reaction of exo-glucal with nitrone

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Date

2008

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Abstract

With microwave irradiation, the efficiency of the 1,3-dipolar cycloaddition of exo-glucal (1) with nitrones 2 was remarkably improved, and the yield of the microwave assisted reaction in a seamless pressure vial at 200 °C for 2 min could be up to 96%, providing a practical and convenient method for preparing spiro-isoxazolidine glycosides which are very important intermediates for synthesizing various C-glycosides possessing functional groups.

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Keywords

1,3-Dipolar cycloaddition, Exo-glycal, Microwave assisted, Nitrone, Spiro-isoxazolidine glycoside

Citation

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https://dspace-test.anu.edu.au/handle/1885/733746715

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DevOps Pure Testing

Source

Chinese Journal of Organic Chemistry

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Article

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